The basic principle of miniature high-pressure reactor is to make use of high temperature and high pressure environment to make the reacting substances react under relatively ideal reaction conditions by controlling the temperature and pressure and other factors.The equipment usually consists of kettle,heating system,pressure control system,stirring system and safety control system.The kettle is the container for the reacting substances and is usually made of materials that are resistant to high pressure,high temperature and corrosion.The heating system provides heat through heaters to bring the kettle temperature to the desired reaction temperature.The pressure control system regulates the pressure inside the kettle to realise the demand under different reaction conditions.The stirring system is used to promote the mixing and mass transfer of the reacting substances and increase the reaction speed.The safety control system monitors and protects the safety of the reaction process.
Miniature high pressure reactor has a wide range of applications in chemical experiments.It can carry out organic synthesis reactions,such as esterification and oxidation,under high temperature and high pressure conditions.These reactions usually require a certain pressure and temperature to be carried out effectively,and it can provide these conditions.Secondly,it can also be used for the study of catalytic reactions and the preparation of catalysts.In catalytic reactions,the reaction conditions have a great influence on the reaction rate and selectivity,and it can provide the control of the reaction conditions,which is beneficial to the study of the reaction mechanism and optimisation of the reaction parameters.In addition,it can also be used for the storage and delivery of high-pressure synthesis gas,which has important application value in petrochemical and other fields.
Miniature high-pressure reactor is widely used in chemical experiments,mainly including the following aspects:
Catalytic research:Miniature autoclaves can be used for the screening and evaluation of catalysts and the optimisation of catalytic reaction conditions.In catalysis research,the performance of catalyst can be studied by changing the conditions of reaction temperature,pressure and reaction time.
Material synthesis:It is used to synthesise new materials,such as nanomaterials,composites,polymers and so on.High-pressure conditions help to improve the purity and properties of materials.
Organic synthesis:In organic chemistry,miniature high-pressure reactor can be used to carry out addition reaction,elimination reaction,rearrangement reaction,redox reaction,etc.,especially in the occasions where higher pressure is needed to promote the reaction.
Chemical process development:In the early stages of chemical process development,the use of micro high-pressure reactors can quickly assess the feasibility of new processes,reduce the consumption of raw materials,and lower research and development costs.
Process safety research:Through the miniature autoclave,the extreme conditions in actual production can be simulated to study the safety of chemical reactions and provide safe operating parameters for industrial production.
Environmental protection:It is used to study the treatment and degradation process of pollutants,such as wastewater treatment,exhaust gas treatment,etc.The treatment efficiency can be improved under high pressure conditions.
Biochemical industry:In the field of biochemical industry,miniature high pressure reactor can be used in enzyme catalysed reaction,cell culture,biological transformation and other processes,high pressure can improve the conversion rate of biological reaction.
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