glass reactor,jacketed glass reactor,glass reactor vessel
The lift-up autoclave reactor is a common piece of laboratory equipment that is widely used in the fields of chemistry,pharmacy,biology and materials science.It enables research at high temperatures and pressures,facilitating experiments in these fields.The up and down movable stirring system allows easy installation and removal of the stirrer without opening the reactor.It consists of reactor body,electric heater,stirring and speed regulating mechanism,liquid level indicator,temperature controller,safety release valve and other parts.As a result of applying high pressure and high temperature to the specimen chamber,a chemical reaction is generated,which changes ordinary substances under different degrees of dissociation,thus completing the experimental purpose.Clean gases or liquids are fed into the test subject through pipes and the reaction is carried out under the required temperature and pressure by submerging or injecting,etc.
Structural characteristics:
Lifting high pressure reactor usually consists of kettle body,stirring system,heating and cooling system,sealing device,safety device and so on.
The kettle body is usually made of high-strength,corrosion-resistant materials,such as stainless steel,titanium alloy and so on.
The stirring system can be lifted and lowered for easy replacement and maintenance.
Lifting and lowering stirring system:
The stirrer can move up and down in the kettle through the lifting device,which is convenient for material mixing and reaction.
The lifting and stirring system can reduce the sealing wear between the stirring shaft and kettle body and prolong the service life of the equipment.
Heating and cooling system:
Reactor kettles are usually equipped with jacketed or built-in heating elements for heating and cooling systems for cooling.
The heating and cooling systems should be designed to ensure uniform temperature distribution and avoid localised overheating or overcooling.
Sealing devices:
The sealing device of the high pressure reactor is crucial,and mechanical seals or graphite packing seals are usually used to ensure no leakage under high temperature and pressure.
Safety devices:
To ensure safe operation,the reactor is equipped with a variety of safety devices,such as safety valves,rupture discs,pressure gauges,thermometers and so on.
Safety valves are used to release excess pressure when the pressure exceeds the set value to prevent the equipment from overpressure explosion.
Control System:
Modern lift-off high pressure reactors are usually equipped with automatic control systems that can precisely control parameters such as temperature,pressure,stirring speed and so on.
Application field:
Lift-up high pressure reactor is widely used in petrochemical,pharmaceutical synthesis,new material research and development,fine chemicals and other fields.
The operation process of the lifting high-pressure reactor:
1.Switch on and add reaction reagents to it.Then,place the reactor in the stand and add the liquid cleaning agent,which avoids exceeding the safety pressure,to the exhaust valve.
2.Next,the electric heater and mixer are activated under the protection of safety devices.As the temperature rises,the reagents gradually undergo a chemical reaction.At this point,the reaction bottle can be observed by looking at the feed port,the sight window or using a non-contact infrared thermometer to observe the situation inside the reaction bottle.
3.After completing the experiment,you need to switch off the electric heater and stirrer,so that the temperature and pressure return to the normal state and stop the air intake.Wait for the reaction kettle to cool down,and then take out the operation,pay attention to avoid stabbing or scalding and other safety accidents.
Lifting high-pressure reactor maintenance methods:
1.Check whether all instruments and their accessories are intact and undamaged in time before operation.
2.Check the connection of heater,temperature controller and round water valve before use.
3.For the use of high-pressure reactor,it is necessary to regularly replace the sealing ring and vacuum degreasing treatment of accessories.
4.After use,the kettle needs to be cleaned and sterilised by pressure doubling if necessary.
5.In order to ensure the test results,it is also necessary to regularly check and calibrate the temperature gauge,pressure gauge and thermocouple and other components.
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