glass reactor,jacketed glass reactor,glass reactor vessel
Single-layer glass reactor is also known as:glass vacuum reactor,extractor,multi-function reactor,can be in constant temperature conditions for a variety of solvent synthesis reaction,the instrument reaction part of the manipulable fully sealed structure,can be used to use the negative pressure of continuous inhalation of a variety of liquids and gases,but also can be done at different temperatures reflux or distillation.In this article,we share with you the problem of single-layer glass reactor assembly.
Single-layer glass reactor is not like double-layer glass reactor that has a sandwich can be passed into the heat and cold source,so to prepare another heat source,generally supporting the purchase of heating bath or more functional thermostatic bath,the material in the reactor for constant temperature heating or refrigeration,if you only need to heat the function of the purchase of the bath can be relatively cheap,if you also need to refrigerate the purchase of a thermostatic bath,the price is relatively high.
Here are the steps of its assembly:
1、Before assembling,we should carefully check whether the accessories are complete according to the packing list,and whether they are complete without damage.
2、according to the illustration of the assembly of stainless steel frame,this is relatively simple,generally large glass reactor with casters at the bottom,on a flat surface to ensure that the four legs are smooth and do not shake can be.
3、bracket uprights on the slider stainless steel multi-purpose clamps can be sliding adjustment,is used to fix the kettle body in different directions of different heights of the bracket and the electrical part of the single-layer kettle is generally two uprights,double-layer is four uprights.
4、According to the use of height,the kettle body bracket is fixed on the vertical bar slider,the glass kettle is put on the bracket,pay attention to ensure that the kettle body is vertical,the semi-circular hoop is inserted into the vertical bar slider,used to fix the kettle neck,the position is correct,then tighten the fixing screws.
5、Stirring rod is fixed in the motor spindle of the tooth ring chuck,stirring rod through the middle of the cover rotating bearing,tighten the connector,and then adjust the position of the motor,pay attention to the vertical through the kettle body of the centre of the circle.
6、Install the electrical box at the top of the right rear upright and tighten the screws,the vacuum gauge is installed at the rear end,tighten the screws can be.
7、The left standard port on the cap is used to insert the serpentine reflux condenser,the right standard port is the charging port to connect the constant pressure funnel,the middle front standard port is the insertion of the thermometer casing port,the kettle cover rear standard port is the multifunctional spare port,the bottom is equipped with a discharge valve,the kettle body lower port connects to the inlet of the circulating liquid,and the upper port connects to the circulating liquid reflux port.
8、the installation of glass instruments must be clean,each interface can be coated with petroleum jelly to prevent the glass hold,and then coated with vacuum grease to enhance airtightness.
9、Fix the universal wheel,turn on the power for stirring,if the stirring is smooth,it means that the debugging has been completed.
Please operate in accordance with specific equipment instructions and operating procedures and under the guidance of a professional.Safety first,ensure that all safety regulations are followed during assembly and use.
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